We have a new methods paper available in Current Protocols in Neuroscience in collaboration with the Roitman Lab and first-authored by Sam Fortin. It describes in detail all the steps required to make fast-scan cyclic voltammetry recordings in freely-moving subjects. Email one of us if you would like a PDF.
Fortin et al (2015). Sampling phasic dopamine signaling with fast-scan cyclic voltammetry in awake, behaving rats. Curr Protoc Neurosci 70:7.25.1-7.25.20. PMID: 25559005